| Citation: | Jiawei Chen, Zhengyu Bao, Yuping Mei. Electrical Calibration for Calvet Type Microcalorimetry. Journal of Earth Science, 2001, 12(3): 232-235.
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The device construction and working principle of Calvet type heat conductive microcalorimetry are generally introduced in this paper. Based on previous work, we design a reactor vessel and its electrical calibration equipment according to our special study systems. The heat constant of our improved microalorimetry is gotten by means of electrical calibration on the basis of Tian's equation. The results gotten by integration method are identical with ones gotten by peak method. It shows that our improved device works well enough to develop further studies.
| Zhang Y, Zeng X, Cheng Y, 1999. Advances in Thermokinetic Research Methods of Chemical Reactions. Chemical Research and Application, 11(2): 132-137 http://en.cnki.com.cn/Article_en/CJFDTOTAL-HXYJ902.003.htm |
| Ingemar W, 2000. Needs for Standards in Isothermal Microcalorimetry. Thermochimica Acta, 347: 73-77 |
| Tang Y, Tian D, Mao Y, 1989. Calibration of High Temperature Calvet Microcalorimeter by the Joule Effect. Earth Science—Journal of China University of Geosciences, 14(3): 271-278 |
| Calvet E, Prat H, 1963. Recent Progress in Microcalorimetry. London: Pergamon Press |
| Tian A, Qin Z, Zeng X, et al, 1981. A Conduction Type Automatic Calorimeter. Chemical Journal of Chinese Universities, 2(2): 244-250 |
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